{"id":8904,"date":"2022-09-08T08:36:17","date_gmt":"2022-09-08T08:36:17","guid":{"rendered":"https:\/\/www.aluminiumceramicfiber.com\/?p=8904"},"modified":"2022-09-08T08:36:31","modified_gmt":"2022-09-08T08:36:31","slug":"purifying-aluminum","status":"publish","type":"post","link":"https:\/\/www.aluminiumceramicfiber.com\/tr\/purifying-aluminum\/","title":{"rendered":"al\u00fcminyumun ar\u0131t\u0131lmas\u0131"},"content":{"rendered":"

\u201cal\u00fcminyumun ar\u0131t\u0131lmas\u0131<\/a>\u201c.<\/p>\n

 <\/p>\n

\"al\u00fcminyumun

al\u00fcminyumun ar\u0131t\u0131lmas\u0131<\/p><\/div>\n

 <\/p>\n

1.1 Sinterleme mekanizmas\u0131 \u00fczerine ara\u015ft\u0131rmalar<\/p>\n

1.1.1 DSC diferansiyel termal analiz<\/p>\n

\u015eekil 4-1, \u00f6l\u00e7\u00fclen DSC-TG e\u011frisini g\u00f6stermektedir. \u015eekildeki ekzotermik tepe noktalar\u0131 146 \u00b0C, 570 \u00b0C, 663 \u00b0C ve 388 \u00b0C; endotermik tepe noktalar\u0131 ise 614 \u00b0C ve 1119 \u00b0C\u2019dir. 146 \u00b0C, poli\u00fcretan k\u00f6p\u00fc\u011f\u00fcn yumu\u015famaya ba\u015flad\u0131\u011f\u0131 s\u0131cakl\u0131kt\u0131r; 570 \u00b0C ise poli\u00fcretan k\u00f6p\u00fc\u011f\u00fcn kokla\u015farak buharla\u015ft\u0131\u011f\u0131 s\u0131cakl\u0131kt\u0131r; 1119 \u00b0C'deki endotermik \u00e7ukur, sinterleme yard\u0131mc\u0131s\u0131 olarak 4wt% CeO\u2082 ilavesinin, bu s\u0131cakl\u0131kta bulamac\u0131n bir s\u0131v\u0131 faz \u00fcretmesine neden oldu\u011funu g\u00f6stermektedir; 1388 \u00b0C'de, s\u0131v\u0131 faz g\u00f6zenekli seramik filtre<\/a> kat\u0131 faz, bu da ekzotermik bir tepe noktas\u0131na yol a\u00e7ar. Kordierit \u00fcretimindeki en belirgin sorun, dar pi\u015firme aral\u0131\u011f\u0131d\u0131r. 1300-1400 \u00b0C'de kordieritin olu\u015fum h\u0131z\u0131 \u00e7ok yava\u015ft\u0131r ve s\u0131cakl\u0131k 1450 \u00b0C'ye ula\u015ft\u0131\u011f\u0131nda kordierit erir ve mullit ile cam g\u00f6vdeye ayr\u0131\u015f\u0131r. 4wt% ceO2 ilavesinin sinterleme s\u0131cakl\u0131\u011f\u0131n\u0131 etkili bir \u015fekilde d\u00fc\u015f\u00fcrd\u00fc\u011f\u00fc ve sinterleme aral\u0131\u011f\u0131n\u0131 geni\u015fletti\u011fi g\u00f6r\u00fclebilir.<\/p>\n

Kordieritin teorik bile\u015fimi 2MgO\u00b72Al\u2082O\u2083\u00b75SiO\u2082 (Mg\u2082Al\u2088Si\u2081\u2083) olup, bunun i\u00e7inde MgO 8, Al\u2082O\u2083 ,9 ve SiO\u2082 ,3't\u00fcr. Kvazi-faz i\u00e7i ikame nedeniyle kimyasal bile\u015fimi genellikle teorik bile\u015fimden farkl\u0131d\u0131r.<\/p>\n

\u201cal\u00fcminyumun ar\u0131t\u0131lmas\u0131<\/a>\u201c.<\/p>\n

MgO-Al\u2082O\u2083-SiO\u2082 sisteminin faz diyagram\u0131 \u00e7emberinde kordieritin konumu \u015eekil 4-2\u2019de g\u00f6sterilmi\u015ftir. Kordieritin erime noktas\u0131 yakla\u015f\u0131k 1465 \u00b0C\u2019dir ve \u0131s\u0131t\u0131ld\u0131\u011f\u0131nda homojen bir \u015fekilde erimeyerek mullit ve s\u0131v\u0131 faza ayr\u0131\u015fmaz. Bu nedenle, kordierit seramik malzemesi \u00e7ok y\u00fcksek s\u0131cakl\u0131klarda kullan\u0131lamaz. Kordieritin, d\u00fc\u015f\u00fck s\u0131cakl\u0131k kordieriti ve y\u00fcksek s\u0131cakl\u0131k kordieriti olmak \u00fczere iki homojen \u00e7ok fazl\u0131 \u00e7e\u015fidi vard\u0131r. Hint ta\u015f\u0131 olarak da bilinen y\u00fcksek s\u0131cakl\u0131k kordieriti, alt\u0131gen kristal sistemine aittir; d\u00fc\u015f\u00fck s\u0131cakl\u0131k kordieriti ise genellikle Dong Qingshi olarak bilinir. Ortorombik sisteme aittir. MgO-Ab2O3-SiO2 sisteminin faz diyagram\u0131ndan da g\u00f6r\u00fclebilece\u011fi gibi, kordierit sinterleme s\u0131cakl\u0131k aral\u0131\u011f\u0131 \u00e7ok dard\u0131r ve yapay sentezdeki en b\u00fcy\u00fck zorluk, y\u00fcksek safl\u0131kta kordierit seramikleri elde etmek i\u00e7in ara fazlar\u0131 (kuvars faz\u0131, spinel faz\u0131) nas\u0131l kontrol edilece\u011fidir.<\/p>\n

\u015eekil 4-3\u2019ten de g\u00f6r\u00fclebilece\u011fi \u00fczere, CeO\u2082 ilavesi yap\u0131lmam\u0131\u015f sinterlenmi\u015f \u00fcr\u00fcnde kuvars ve spinel gibi az say\u0131da ara faz bulunmaktad\u0131r; ancak %4 a\u011f\u0131rl\u0131k\u00e7a CeO\u2082 ilavesinden sonra ara faz i\u00e7eri\u011fi \u00f6nemli \u00f6l\u00e7\u00fcde azalmakta ve neredeyse tamamen ortadan kalkmaktad\u0131r ki bu durum idealdir. Sinterleme etkisi, sinterleme yard\u0131mc\u0131s\u0131 olarak belirli miktarda CeO\u2083 ilavesinin sinterleme etkisini \u00f6nemli \u00f6l\u00e7\u00fcde iyile\u015ftirebilece\u011fini g\u00f6stermektedir.<\/p>","protected":false},"excerpt":{"rendered":"

“purifying aluminum“.     1.1 Research on sintering mechanism 1.1.1 DSC differential thermal analysis Figure 4-1 shows the measured DSC-TG curve. The exothermic peaks in the figure are 146\u00b0C, 570\u00b0C, 663\u00b0C, and 388\u00b0C, and the endothermic peaks are 614\u00b0C and 1119\u00b0C. 146\u00b0C is the temperature at which the polyurethane foam begins to soften: 570\u00b0C is […]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[86],"tags":[46],"class_list":["post-8904","post","type-post","status-publish","format-standard","hentry","category-blog","tag-ceramic-foam-filter"],"yoast_head":"\npurifying aluminum, ceramic foam filter, porous ceramic filter<\/title>\n<meta name=\"description\" content=\""purifying aluminum". the liquid phase precipitated into the porous ceramic filter solid phase, resulting in an exothermic peak.\" \/>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" 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